Technology Process of 5,6-dimethoxy-1-phenyl-isoquinoline
There total 13 articles about 5,6-dimethoxy-1-phenyl-isoquinoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium acetate; sodium acetate;
In
tetrahydrofuran; water;
at 50 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2012.02.045
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere
2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 0.5 h / 50 °C / Inert atmosphere
3: sodium periodate / tetrahydrofuran; water / 0.17 h / 50 °C / Inert atmosphere
4: ammonium acetate; sodium acetate / tetrahydrofuran; water / 0.33 h / 50 °C / Inert atmosphere
With
sodium periodate; osmium(VIII) oxide; ammonium acetate; water; sodium acetate; 4-methylmorpholine N-oxide; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2012.02.045
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium periodate / tetrahydrofuran; water / 0.17 h / 50 °C / Inert atmosphere
2: ammonium acetate; sodium acetate / tetrahydrofuran; water / 0.33 h / 50 °C / Inert atmosphere
With
sodium periodate; ammonium acetate; sodium acetate;
In
tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2012.02.045
