N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

Base Information

Chemical Name:N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane
CAS No.:693274-36-1
Molecular Formula:C₁₆H₂₆N₂
Molecular Weight:246.396
Hs Code.:

Synonyms:N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

Suppliers and Price of N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

There total 3 articles about N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 227315-17-5
N,N'-bis-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

: 693274-36-1
N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; for 24h; under 2280.15 Torr;
DOI:10.1016/j.tet.2004.02.025

Reference yield:

: 138812-17-6
N,N'-bis<(S)-1-phenylethyl>ethanediimine

: 693274-36-1
N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / bis-(cyclopentadienyl)zirconium dichloride; n-butylmagnesium chloride / diethyl ether / 44 h / 20 °C

2: 47 percent / H₂ / Pd(OH)2/C / methanol / 24 h / 2280.15 Torr

With zirconocene dichloride; hydrogen; butyl magnesium bromide; palladium dihydroxide; In methanol; diethyl ether;
DOI:10.1016/j.tet.2004.02.025

Reference yield:

: 138812-19-8
(4R,5R)-N₄,N₅-bis((S)-1-phenylethyl)octa-1,7-diene-4,5-diamine

: 693274-36-1
N-[(S)-1'-phenylethyl]-(1R,2R,4R,5R)-1,2-diamino-4,5-dimethyl-cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / bis-(cyclopentadienyl)zirconium dichloride; n-butylmagnesium chloride / diethyl ether / 44 h / 20 °C

2: 47 percent / H₂ / Pd(OH)2/C / methanol / 24 h / 2280.15 Torr

With zirconocene dichloride; hydrogen; butyl magnesium bromide; palladium dihydroxide; In methanol; diethyl ether;
DOI:10.1016/j.tet.2004.02.025