4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

Base Information

Chemical Name:4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide
CAS No.:1306720-37-5
Molecular Formula:C₂₁H₂₄N₄O₄S
Molecular Weight:428.512
Hs Code.:

Synonyms:4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

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Technology Process of 4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

There total 4 articles about 4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 1306723-10-3
4-(4-amino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

: 814-68-6,25189-84-8
acryloyl chloride

: 1306720-37-5
4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 3173-56-6
benzyl isothiocyanate

: 1306720-37-5
4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2 h / 50 °C

2: ammonium chloride; iron / ethanol; water / 3 h / 80 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With pyridine; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1306723-09-0
4-(4-nitro-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

: 1306720-37-5
4-(4-acryloylamino-benzenesulfonyl)-piperazine-1-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; iron / ethanol; water / 3 h / 80 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; In ethanol; water; N,N-dimethyl-formamide;