1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

Base Information

Chemical Name:1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide
CAS No.:1620922-84-0
Molecular Formula:C₄₃H₆₇N₄O₆*I
Molecular Weight:862.933
Hs Code.:

Synonyms:1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

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Chemical Property of 1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

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Technology Process of 1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

There total 6 articles about 1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1620922-83-9
1,3-bis(2,6-diisopropyl-4-hydroxyphenyl)imidazolium chloride

: 167479-01-8
tert-butyl (3-iodopropyl)carbamate

: 1620922-84-0
1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201300903

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1620922-84-0
1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium iodide; tert.-butylhydroperoxide / acetonitrile; water / 6.25 h / 70 °C

2.1: ammonium chloride / acetone / 0.5 h / Inert atmosphere; Schlenk technique

2.2: 5 h / Inert atmosphere; Schlenk technique

3.1: sulfuric acid / water; diethyl ether / 12.17 h / Inert atmosphere; Schlenk technique

4.1: formic acid / ethanol / 8 h / Inert atmosphere; Schlenk technique; Heating

5.1: dimethyl sulfoxide / 48 h / 45 - 50 °C / Inert atmosphere; Schlenk technique

6.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere; Schlenk technique

With tert.-butylhydroperoxide; formic acid; sulfuric acid; potassium carbonate; ammonium chloride; potassium iodide; In diethyl ether; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/adsc.201300903

Reference yield:

: 91563-76-7
1,3-diisopropyl-2-nitrobenzene

: 1620922-84-0
1,3-bis(4-{3-[(tert-butoxycarbonyl)amino]propyloxy}-2,6-diisopropylphenyl)imidazolium iodide

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonium chloride / acetone / 0.5 h / Inert atmosphere; Schlenk technique

1.2: 5 h / Inert atmosphere; Schlenk technique

2.1: sulfuric acid / water; diethyl ether / 12.17 h / Inert atmosphere; Schlenk technique

3.1: formic acid / ethanol / 8 h / Inert atmosphere; Schlenk technique; Heating

4.1: dimethyl sulfoxide / 48 h / 45 - 50 °C / Inert atmosphere; Schlenk technique

5.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere; Schlenk technique

With formic acid; sulfuric acid; potassium carbonate; ammonium chloride; In diethyl ether; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1002/adsc.201300903