benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate

Base Information

Chemical Name:benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate
CAS No.:1236182-10-7
Molecular Formula:C₁₉H₂₅NO₅
Molecular Weight:347.411
Hs Code.:

Synonyms:benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate

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Technology Process of benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate

There total 1 articles about benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1445-45-0
Trimethyl orthoacetate

: 1236182-09-4
benzyl (4R)-4-(1-hydroxyallyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1236182-10-7
benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: With propionic acid; In 5,5-dimethyl-1,3-cyclohexadiene; for 18h; optical yield given as %de; stereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol101252y

Reference yield: 96.0%

: 1236182-10-7
benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1236182-11-8
(S,E)-5-(3-(benzyloxycarbonyl)-2,2-dimethyloxazolidin-4-yl)pent-4-enoic acid

Guidance literature:: benzyl (S,E)-4-(5-methoxy-5-oxopent-1-enyl)-2,2-dimethyloxazolidine-3-carboxylate; With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; methanol; water; ethyl acetate; at 0 ℃; pH=3; Inert atmosphere;
DOI:10.1021/ol101252y