(E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

Base Information

Chemical Name:(E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole
CAS No.:1392500-13-8
Molecular Formula:C₃₈H₅₃N₃O₁₃
Molecular Weight:759.851
Hs Code.:

Synonyms:(E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

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Chemical Property of (E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

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Technology Process of (E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

There total 7 articles about (E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1392500-07-0
5,5'-(2-azidopropane-1,3-diyl)bis(oxy)bis(2,2-dimethyl-1,3-dioxane)

: 1392500-12-7
(E)-1,2-bis(methoxymethoxy)-4-(3-(methoxymethoxy)-5-(prop-2-ynyloxy)styryl)benzene

: 1392500-13-8
(E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.06.019

Reference yield:

: 1392500-09-2
C₁₂H₁₄O₄

: 1392500-13-8
(E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,6-dimethylpyridine; carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: 3 h / 100 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

4.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 6 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; copper(ll) sulfate pentahydrate; carbon tetrabromide; sodium hydride; sodium L-ascorbate; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; mineral oil; tert-butyl alcohol; 3.1: Horner-Wadsworth-Emmons Wittig olefination / 3.2: Horner-Wadsworth-Emmons Wittig olefination;
DOI:10.1016/j.bmcl.2012.06.019

Reference yield:

: 1392500-08-1
diethyl 3-(methoxymethoxy)-5-(prop-2-ynyloxy)benzylphosphonate

: 1392500-13-8
(E)-1-(1,3-bis(2,2-dimethyl-1,3-dioxan-5-yloxy)propan-2-yl)-4-((3-(3,4-bis(methoxymethoxy)styryl)-5-(methoxymethoxy)phenoxy)methyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 6 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; sodium hydride; sodium L-ascorbate; In tetrahydrofuran; water; mineral oil; tert-butyl alcohol; 1.1: Horner-Wadsworth-Emmons Wittig olefination / 1.2: Horner-Wadsworth-Emmons Wittig olefination;
DOI:10.1016/j.bmcl.2012.06.019