1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

Base Information

Chemical Name:1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide
CAS No.:78157-94-5
Molecular Formula:C₁₁H₇N₃O₅S
Molecular Weight:293.26
Hs Code.:

Synonyms:1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

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Chemical Property of 1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

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Technology Process of 1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

There total 3 articles about 1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3529-82-6
3-nitrophenyl isothiocyanate

: ethyl sodiocyanopyruvate

: 78157-94-5
1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

Guidance literature:: In N,N-dimethyl-formamide; for 10h; Ambient temperature;

Reference yield: 90.0%

: 3-Cyano-3-(3-nitro-phenylthiocarbamoyl)-2-oxo-propionic acid; compound with N,N-dimethyl-formamide

: 78157-94-5
1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

Guidance literature:: With sodium hydroxide; In water; for 0.166667h; Ambient temperature;

Reference yield:

: 3529-82-6
3-nitrophenyl isothiocyanate

: 78157-94-5
1-(3-Nitro-phenyl)-4,5-dioxo-2-thioxo-pyrrolidine-3-carboxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / dimethylformamide / Ambient temperature

2: 90 percent / 2.5percent aq. NaOH / H₂O / 0.17 h / Ambient temperature

With sodium hydroxide; In water; N,N-dimethyl-formamide;