Technology Process of C31H33N7O3
There total 8 articles about C31H33N7O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C21H20N4O2;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 5 - 10 ℃;
for 0.5h;
Inert atmosphere;
C11H17N3O4S;
In
N,N-dimethyl-formamide; mineral oil;
at 60 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / methanol; tetrahydrofuran / 1.5 h / 20 °C / 2250.23 Torr
2.1: caesium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium(0) / 18 h / 100 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 - 10 °C / Inert atmosphere
3.2: 60 °C
With
tris-(dibenzylideneacetone)dipalladium(0); hydrogen; sodium hydride; caesium carbonate; XPhos;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: caesium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium(0) / 18 h / 100 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 5 - 10 °C / Inert atmosphere
2.2: 60 °C
With
tris-(dibenzylideneacetone)dipalladium(0); sodium hydride; caesium carbonate; XPhos;
In
N,N-dimethyl-formamide; mineral oil;