C₄₂H₄₅N₃O₁₂

Base Information

Chemical Name:C₄₂H₄₅N₃O₁₂
CAS No.:1262887-48-8
Molecular Formula:C₄₂H₄₅N₃O₁₂
Molecular Weight:783.832
Hs Code.:

C<sub>42</sub>H<sub>45</sub>N<sub>3</sub>O<sub>12</sub>

Synonyms:C₄₂H₄₅N₃O₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₂H₄₅N₃O₁₂

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Technology Process of C₄₂H₄₅N₃O₁₂

There total 13 articles about C₄₂H₄₅N₃O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: C₄₄H₄₇N₃O₁₂

: 1262887-48-8
C₄₂H₄₅N₃O₁₂

Guidance literature:: With trifluoroacetic acid; at -5 - 20 ℃; for 4h; Industry scale;

Reference yield:

: 55682-48-9
1,6-anhydro-2-azido-3,4-di-O-benzyl-2-deoxy-D-glucopyranose

: 1262887-48-8
C₄₂H₄₅N₃O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1: boron trifluoride diethyl etherate / dichloromethane / 3 h / -10 - 20 °C / Industry scale; Inert atmosphere

2: hydrazinium monoacetate / N,N-dimethyl-formamide / 3 h / 20 °C / Industry scale

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 20 °C / Inert atmosphere; Industry scale

4: triethylsilyl trifluoromethyl sulfonate / dichloromethane / 2 h / -40 °C / Industry scale; Inert atmosphere

5: trifluoroacetic acid / 4 h / -5 - 20 °C / Industry scale

With boron trifluoride diethyl etherate; triethylsilyl trifluoromethyl sulfonate; hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1262887-48-8
C₄₂H₄₅N₃O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium tetrahydroborate / acetonitrile / 16 h / 40 °C / Molecular sieve

2.1: sodium methylate / methanol / 3 h / 50 °C

3.1: (1S)-10-camphorsulfonic acid / 2 h / 50 °C

4.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

4.2: 0.5 h

5.1: trifluoroacetic acid; water / dichloromethane / 0 °C

6.1: tetrabutyl-ammonium chloride; sodium hydrogencarbonate; sodium hypochlorite; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / ethyl acetate / 16 h / 20 °C

7.1: triethylamine; dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 16 h / 20 °C

8.1: triethylsilyl trifluoromethyl sulfonate / dichloromethane / 2 h / -40 °C / Industry scale; Inert atmosphere

9.1: trifluoroacetic acid / 4 h / -5 - 20 °C / Industry scale

With sodium hypochlorite; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; (1S)-10-camphorsulfonic acid; tetrabutyl-ammonium chloride; water; triethylsilyl trifluoromethyl sulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium bromide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile;