C₂₈H₃₆N₆O₈

Base Information

Chemical Name:C₂₈H₃₆N₆O₈
CAS No.:1295471-34-9
Molecular Formula:C₂₈H₃₆N₆O₈
Molecular Weight:584.629
Hs Code.:

C<sub>28</sub>H<sub>36</sub>N<sub>6</sub>O<sub>8</sub>

Synonyms:C₂₈H₃₆N₆O₈

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Chemical Property of C₂₈H₃₆N₆O₈

Chemical Property:

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Technology Process of C₂₈H₃₆N₆O₈

There total 36 articles about C₂₈H₃₆N₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1295471-30-5
C₂₀H₃₀N₆O₆

: 438187-09-8
2-hydroxy-6-methyl-benzoic acid cyanomethyl ester

: 1295471-34-9
C₂₈H₃₆N₆O₈

Guidance literature:: 2-hydroxy-6-methyl-benzoic acid cyanomethyl ester; With potassium carbonate; In ISOPROPYLAMIDE; at 20 ℃; for 1h; Inert atmosphere;

C₂₀H₃₀N₆O₆; In ISOPROPYLAMIDE; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-59-8
C₁₇H₂₂N₄O₆

: 1295471-34-9
C₂₈H₃₆N₆O₈

Guidance literature:: Multi-step reaction with 13 steps

1.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

3.1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

5.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6.1: CSA / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

7.1: pyrographite; triethylamine / tetrahydrofuran / 0.25 h / -46 °C / Inert atmosphere

8.1: -46 - 20 °C

9.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

10.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone / 2 h / 20 °C

11.1: sodium periodate / tetrahydrofuran; water / 3 h / 20 °C

12.1: water; trifluoroacetic acid / acetonitrile / 0.75 h / 0 - 20 °C

13.1: potassium carbonate / ISOPROPYLAMIDE / 1 h / 20 °C / Inert atmosphere

13.2: 0.17 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; diisobutylaluminium hydride; potassium carbonate; pyrographite; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-20-3
C₃₃H₃₈N₄O₅Si

: 1295471-34-9
C₂₈H₃₆N₆O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

3.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

4.1: CSA / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: pyrographite; triethylamine / tetrahydrofuran / 0.25 h / -46 °C / Inert atmosphere

6.1: -46 - 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

8.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone / 2 h / 20 °C

9.1: sodium periodate / tetrahydrofuran; water / 3 h / 20 °C

10.1: water; trifluoroacetic acid / acetonitrile / 0.75 h / 0 - 20 °C

11.1: potassium carbonate / ISOPROPYLAMIDE / 1 h / 20 °C / Inert atmosphere

11.2: 0.17 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium periodate; osmium(VIII) oxide; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; diisobutylaluminium hydride; potassium carbonate; pyrographite; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; ISOPROPYLAMIDE; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;
DOI:10.1002/anie.201008079