1-deuterium-p-tolylacetylene

Base Information

Chemical Name:1-deuterium-p-tolylacetylene
CAS No.:92985-68-7
Molecular Formula:C₉H₈
Molecular Weight:117.155
Hs Code.:

Synonyms:1-deuterium-p-tolylacetylene

Suppliers and Price of 1-deuterium-p-tolylacetylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-deuterium-p-tolylacetylene

Chemical Property:

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Technology Process of 1-deuterium-p-tolylacetylene

There total 5 articles about 1-deuterium-p-tolylacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 766-97-2
4-n-methylphenylacetylene

: 92985-68-7
1-deuterium-p-tolylacetylene

Guidance literature:: With water-d2; triethylamine; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201700282

Reference yield: 25.0%

: 3240-11-7
Phenylacetylene-d1

: 766-97-2
4-n-methylphenylacetylene

: 92985-68-7
1-deuterium-p-tolylacetylene

: 536-74-3
phenylacetylene

Guidance literature:: With [(tris(3,5-dimethylpyrazolylmethyl)amine)Cu]PF₆; at 40 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201303737

Reference yield:

: 122-00-9
para-methylacetophenone

: 92985-68-7
1-deuterium-p-tolylacetylene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) PCl₅; 2.) KOH / 1.) reflux; 2.) Me₂SO, H₂O

2: D₂O / diethyl ether / Ambient temperature

With potassium hydroxide; phosphorus pentachloride; water-d2; In diethyl ether;
DOI:10.1021/ja00305a019