[1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

Base Information

Chemical Name:[1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine
CAS No.:174474-60-3
Molecular Formula:C₂₈H₅₀N₂OSi
Molecular Weight:458.803
Hs Code.:

Synonyms:[1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

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Technology Process of [1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

There total 1 articles about [1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96045-13-5
1-bromo-8-[(tert-butyldimethylsilyl)oxy]octane

: [1-Methyl-pent-(E)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

: 174474-60-3
[1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) -45 deg C, 2 h;
DOI:10.1021/ja951422p

Reference yield:

: 174474-60-3
[1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

: 16725-53-4
(Z)-9-tetradecen-1-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: LDA / diethyl ether / 1 h / 0 °C

2: AcOH / tetrahydrofuran; H₂O / 3 h / 25 °C

3: pyridine, DMAP / CH₂Cl₂ / 1 h / 25 °C

With pyridine; dmap; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/ja951422p

Reference yield:

: 174474-60-3
[1-Butyl-10-(tert-butyl-dimethyl-silanyloxy)-dec-(Z)-ylidene]-(2-phenyl-aziridin-1-yl)-amine

: 35153-15-2
(Z)-9-tetradecen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: LDA / diethyl ether / 1 h / 0 °C

2: AcOH / tetrahydrofuran; H₂O / 3 h / 25 °C

With acetic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; water;
DOI:10.1021/ja951422p