C₂₄H₃₀O₅Si

Base Information

Chemical Name:C₂₄H₃₀O₅Si
CAS No.:1612775-33-3
Molecular Formula:C₂₄H₃₀O₅Si
Molecular Weight:426.585
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>5</sub>Si

Synonyms:C₂₄H₃₀O₅Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₀O₅Si

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Technology Process of C₂₄H₃₀O₅Si

There total 1 articles about C₂₄H₃₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₂₄H₃₂O₅Si

: 1612775-33-3
C₂₄H₃₀O₅Si

Guidance literature:: With N-iodo-succinimide; tetra-(n-butyl)ammonium iodide; In dichloromethane; at 20 ℃; for 21h; Inert atmosphere;
DOI:10.1021/ol501446w

Reference yield: 84.0%

: 1612775-33-3
C₂₄H₃₀O₅Si

: 1005-56-7
phenylcarbonochloridothioate

: 1612775-34-4
C₃₁H₃₄O₆SSi

Guidance literature:: With dmap; In acetonitrile; at 0 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1021/ol501446w

Reference yield:

: 1612775-33-3
C₂₄H₃₀O₅Si

: 1612775-37-7
C₂₆H₃₅NO₄Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap / acetonitrile / 0.67 h / 0 °C / Inert atmosphere

2.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / Inert atmosphere; Reflux

3.1: trimethylaluminum / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 1.5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C / Inert atmosphere

With dmap; 2,2'-azobis(isobutyronitrile); trimethylaluminum; tri-n-butyl-tin hydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane; toluene; acetonitrile; 2.1: |Barton-McCombie Deoxygenation;
DOI:10.1021/ol501446w