benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Base Information

Chemical Name:benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside
CAS No.:93661-20-2
Molecular Formula:C₄₇H₅₀O₁₁
Molecular Weight:790.907
Hs Code.:

Synonyms:benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Suppliers and Price of benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

There total 5 articles about benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 93661-18-8
benzyl 2,3,6-tri-O-benzyl-4-O-β-D-glucopyranosyl-β-D-galactopyranoside

: 93661-20-2
benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; for 3h; Ambient temperature;
DOI:10.1016/0008-6215(84)85204-0

Reference yield:

: 74801-06-2
benzyl 2,3-di-O-benzyl-4,6-ol-β-D-galactopyranoside

: 93661-20-2
benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / tetrabutylammonium hydrogensulfate, 5 percent sodium hydroxide / CH₂Cl₂ / 10 h / Heating

2: mercuric cyanide / benzene; nitromethane / 17 h / 45 °C

3: M sodium methoxide / methanol / 3 h / Ambient temperature

4: 90 percent / p-toluenesulfonic acid monihydrate / acetonitrile / 3 h / Ambient temperature

With sodium hydroxide; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; mercury(II) cyanide; toluene-4-sulfonic acid; In methanol; nitromethane; dichloromethane; acetonitrile; benzene;
DOI:10.1016/0008-6215(84)85204-0

Reference yield:

: 57783-81-0
Benzyl 2,3,6-tri-O-benzyl-β-D-galactopyranoside

: 93661-20-2
benzyl 2,3,6-tri-O-benzyl-4-O-(4,6-O-benzylidene-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: mercuric cyanide / benzene; nitromethane / 17 h / 45 °C

2: M sodium methoxide / methanol / 3 h / Ambient temperature

3: 90 percent / p-toluenesulfonic acid monihydrate / acetonitrile / 3 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; In methanol; nitromethane; acetonitrile; benzene;
DOI:10.1016/0008-6215(84)85204-0