3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid

Base Information

• Chemical Name: 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid
• CAS No.: 1544500-13-1
• Molecular Formula: C₂₅H₁₈O₁₂
• Molecular Weight: 510.411
• Mol file: 1544500-13-1.mol

Synonyms:3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid

Chemical Property of 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid

Chemical Property:

Purity/Quality:

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Technology Process of 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid

There total 1 articles about 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3,5-bis(1-methoxy-3,5-benzene dicarboxylic acid)benzoic acid dimethyl ester (1544500-17-5) → 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid (1544500-13-1)

Guidance literature:

3,5-bis(1-methoxy-3,5-benzene dicarboxylic acid)benzoic acid dimethyl ester; With sodium hydroxide; In methanol; water; Reflux;

With hydrogenchloride; In water;

DOI:10.1039/c3tc32001d

Reference yield:

N,N-dimethyl acetamide (127-19-5,116057-81-9) + 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid (1544500-13-1) + zinc(II) chloride (7646-85-7,24359-56-6) → N,N'-dimethylacetamide

Guidance literature:

N,N-dimethyl acetamide; 3,5-bis(1-methoxy-3,5-benzene dicarboxylicacid)benzoic acid; zinc(II) chloride; With air; In methanol; at 20 ℃; for 0.166667h;

In methanol; at 90 ℃; for 72h; Sealed tube;

DOI:10.1039/c3tc32001d

upstream raw materials:

3,5-bis(1-methoxy-3,5-benzene dicarboxylic acid)benzoic acid dimethyl ester