bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

Base Information

Chemical Name:bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate
CAS No.:1093260-71-9
Molecular Formula:C₂₄H₂₄ClFN₂O₇
Molecular Weight:506.915
Hs Code.:

Synonyms:bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

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Chemical Property of bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

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Technology Process of bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

There total 5 articles about bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 770719-09-0
3-chloro-5-[(2,3-difluoro-6-nitrophenyl)oxy]benzonitrile

: 541-16-2
t-butyl malonate

: 1093260-71-9
bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

Guidance literature:: t-butyl malonate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

3-chloro-5-[(2,3-difluoro-6-nitrophenyl)oxy]benzonitrile; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 3h;
DOI:10.1021/jm301294g

Reference yield:

: 473923-97-6
3-chloro-5-hydroxybenzonitrile

: 1093260-71-9
bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C

With sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1021/jm301294g

Reference yield:

: 771-69-7
2,3,4-trifluoronitrobenzene

: 1093260-71-9
bis(1,1-dimethylethyl) {3-[(3-chloro-5-cyanophenyl)oxy]-2-fluoro-4-nitrophenyl}propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C

With sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1021/jm301294g