C₄₅H₅₂N₂O₇Si

Base Information

Chemical Name:C₄₅H₅₂N₂O₇Si
CAS No.:886438-09-1
Molecular Formula:C₄₅H₅₂N₂O₇Si
Molecular Weight:761.003
Hs Code.:

C<sub>45</sub>H<sub>52</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₄₅H₅₂N₂O₇Si

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Chemical Property of C₄₅H₅₂N₂O₇Si

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Technology Process of C₄₅H₅₂N₂O₇Si

There total 14 articles about C₄₅H₅₂N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 886437-83-8
C₃₉H₃₈N₂O₇

: 69739-34-0
t-butyldimethylsiyl triflate

: 886438-09-1
C₄₅H₅₂N₂O₇Si

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 351377-71-4
7-bromo-4-methylbenzo[d][1,3]dioxole-5-carbaldehyde

: 886438-09-1
C₄₅H₅₂N₂O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: m-chloroperbenzoic acid / 3 h / 25 - 64 °C

1.2: 78 percent / HCl / 12 h / 0 - 25 °C

2.1: 89 percent / triethylamine; 4-(dimethylamino)pyridine / 12 h / 25 °C

3.1: nBuLi / toluene; tetrahydrofuran / 0.33 h / -78 °C

3.2: 80 percent / toluene; tetrahydrofuran / 50 h / -78 °C

4.1: HCO₂H; triethylamine / Noyori (R,R)-catalyst / dimethylformamide / 24 h / 0 - 40 °C

4.2: diphenylphosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene; dimethylformamide / 24 h / 50 °C

4.3: H₂ / Pd/C / ethyl acetate / 15 h / 25 °C

5.1: acetic acid; NaCNBH₃; MgSO₄ / methanol / 4 h / 0 - 65 °C

6.1: tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

7.1: 84 percent / NaH / dimethylformamide / 2 h / 0 - 25 °C

8.1: 90 percent / HCl / dioxane / 72 h / 0 - 25 °C

9.1: 85 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride; triethylamine / CH₂Cl₂ / 24 h / 0 - 25 °C

10.1: 90 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; buffer solution / CH₂Cl₂ / 0.5 h / 25 °C / pH 7

11.1: 61 percent / Cu(OTf)2 / benzene / 0.25 h / 85 °C

12.1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 5 h / 25 °C

13.1: 93 percent / tributyltin hydride; acetic acid / [(PPh₃)2PdCl₂] / 1 h / 0 - 25 °C

14.1: CHF₂COOH; MgSO₄ / benzene / 0.75 h / 100 °C

15.1: 100 percent / triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

With hydrogenchloride; Difluoroacetic acid; dmap; n-butyllithium; formic acid; buffer solution; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; copper(II) bis(trifluoromethanesulfonate); sodium hydride; sodium cyanoborohydride; magnesium sulfate; Dess-Martin periodane; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-triphenylphosphine-palladium(II) chloride; ((1R,2R)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)ruthenium chloride(I) (4-cymene); In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1002/anie.200503983

Reference yield:

: 886438-05-7
7-[2-benzyloxy-1-(2,2-dimethoxy-ethylamino)-ethyl]-4-methyl-benzo[1,3]dioxol-5-ol

: 886438-09-1
C₄₅H₅₂N₂O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1: 84 percent / NaH / dimethylformamide / 2 h / 0 - 25 °C

2: 90 percent / HCl / dioxane / 72 h / 0 - 25 °C

3: 85 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride; triethylamine / CH₂Cl₂ / 24 h / 0 - 25 °C

4: 90 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; buffer solution / CH₂Cl₂ / 0.5 h / 25 °C / pH 7

5: 61 percent / Cu(OTf)2 / benzene / 0.25 h / 85 °C

6: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 5 h / 25 °C

7: 93 percent / tributyltin hydride; acetic acid / [(PPh₃)2PdCl₂] / 1 h / 0 - 25 °C

8: CHF₂COOH; MgSO₄ / benzene / 0.75 h / 100 °C

9: 100 percent / triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

With hydrogenchloride; Difluoroacetic acid; buffer solution; tri-n-butyl-tin hydride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; copper(II) bis(trifluoromethanesulfonate); sodium hydride; magnesium sulfate; Dess-Martin periodane; acetic acid; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1002/anie.200503983