7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester

Base Information

• Chemical Name: 7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester
• CAS No.: 838872-55-2
• Molecular Formula: C₁₆H₁₇NO₄
• Molecular Weight: 287.315

Synonyms:7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester

Chemical Property of 7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester

Chemical Property:

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Technology Process of 7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester

There total 1 articles about 7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

(2-iodoethyl)(1-methoxy-4-oxocyclohexa-2,5-dienyl)carbamic acid phenyl ester (838872-53-0) → 7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester (838872-55-2)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; Heating;

DOI:10.1021/ol047977j

Reference yield: 86.0%

7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester (838872-55-2) → 5-hydroxy-2,3-dihydroindole-1-carboxylic acid phenyl ester

Guidance literature:

With toluene-4-sulfonic acid; In chloroform;

DOI:10.1021/ol047977j

Reference yield:

7a-methoxy-5-oxo-2,3,3a,4,5,7a-hexahydroindole-1-carboxylic acid phenyl ester (838872-55-2) → C16H19NO4

Guidance literature:

With sodium tetrahydroborate; cerium(III) chloride; In methanol; for 1h;

DOI:10.1021/jo7026307

upstream raw materials:

(2-iodoethyl)(1-methoxy-4-oxocyclohexa-2,5-dienyl)carbamic acid phenyl ester

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