4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide

Base Information

• Chemical Name: 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide
• CAS No.: 120633-81-0
• Molecular Formula: C₁₈H₂₀BrN₃O₈
• Molecular Weight: 486.276

Synonyms:4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide

Chemical Property of 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide

There total 2 articles about 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,4,6-tri-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α/β-D-glucopyranose → 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide (120633-81-0)

Guidance literature:

With titanium(IV) bromide; In dichloromethane; ethyl acetate; Ambient temperature;

Reference yield:

4-O-acetyl-1,6-anhydro-3-O-anisoyl-2-azido-2-deoxy-β-D-glucopyranose → 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide (120633-81-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / trifluoroacetic acid / Ambient temperature

2: 90 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / Ambient temperature

With titanium(IV) bromide; In dichloromethane; ethyl acetate; trifluoroacetic acid;

Reference yield: 54.0%

4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide (120633-81-0) + 1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-galactopyranoside (67817-27-0) → 4-O-(4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-galactopyranose (120633-75-2)

Guidance literature:

With 2,6-di-tert-butyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In toluene; at -20 ℃;

Downstream raw materials:

4-O-(4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-galactopyranose

6-O-acetyl-4-O-(4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl)-2-azido-3-O-benzyl-2-deoxy-α-D-galactopyranosyl bromide

C₄₆H₅₁N₉O₁₇

C₄₈H₅₄BrN₉O₁₈

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 120633-81-0 4,6-di-O-acetyl-3-O-anisoyl-2-azido-2-deoxy-α-D-glucopyranosyl bromide

Send

Send

Metric Ton KG G Pound L ML

Send

Send