Technology Process of C35H22
There total 9 articles about C35H22 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
tetrahydrofuran;
for 20h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methanesulfonic acid / 24 h / 30 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: hydrogenchloride / water; acetic acid / 12 h / Reflux
With
hydrogenchloride; n-butyllithium; methanesulfonic acid;
In
tetrahydrofuran; hexane; water; acetic acid;
DOI:10.5012/bkcs.2011.32.5.1475
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride
2.1: tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 0.5 h / Inert atmosphere
2.2: 80 °C / Inert atmosphere
3.1: methanesulfonic acid / 24 h / 30 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / -78 °C / Inert atmosphere
4.2: -78 - 20 °C / Inert atmosphere
5.1: hydrogenchloride / water; acetic acid / 12 h / Reflux
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; methanesulfonic acid;
In
tetrahydrofuran; hexane; water; acetic acid;
2.1: Suzuki coupling / 2.2: Suzuki coupling;
DOI:10.5012/bkcs.2011.32.5.1475
