Technology Process of 1-pentafluorosulfanyl-4-(trifluoromethylthio)ethynylbenzene
There total 3 articles about 1-pentafluorosulfanyl-4-(trifluoromethylthio)ethynylbenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
[2,2]bipyridinyl; copper(l) iodide; caesium carbonate;
In
1,2-dichloro-ethane;
at 80 ℃;
for 15h;
Schlenk technique;
Inert atmosphere;
Sealed tube;
DOI:10.1002/anie.201307484
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 5 h / 55 °C / Inert atmosphere
2: potassium fluoride / methanol / 20 °C
3: [2,2]bipyridinyl; copper(l) iodide; caesium carbonate / 1,2-dichloro-ethane / 15 h / 80 °C / Schlenk technique; Inert atmosphere; Sealed tube
With
[2,2]bipyridinyl; bis-triphenylphosphine-palladium(II) chloride; potassium fluoride; copper(l) iodide; caesium carbonate; triethylamine;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1002/anie.201307484
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium fluoride / methanol / 20 °C
2: [2,2]bipyridinyl; copper(l) iodide; caesium carbonate / 1,2-dichloro-ethane / 15 h / 80 °C / Schlenk technique; Inert atmosphere; Sealed tube
With
[2,2]bipyridinyl; potassium fluoride; copper(l) iodide; caesium carbonate;
In
methanol; 1,2-dichloro-ethane;
DOI:10.1002/anie.201307484
