2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile

Base Information

Chemical Name:2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile
CAS No.:27334-26-5
Molecular Formula:C₂₁H₂₃N₃
Molecular Weight:317.434
Hs Code.:
European Community (EC) Number:683-772-7
Nikkaji Number:J1.500.644G,J855.563J

Synonyms:2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile;27334-26-5;SCHEMBL17883196;TQP0764;AKOS001482927;1-[4-(Dimethylamino)styryl]-5,5-dimethylcyclohexene-3-ylidenemalononitrile;(E)-2-(3-(4-(dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile;2-[3-[(E)-4-(Dimethylamino)styryl]-5,5-dimethyl-2-cyclohexene-1-ylidene]malononitrile

Suppliers and Price of 2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:317.189197746
Heavy Atom Count:24
Complexity:632

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CC(=CC(=C(C#N)C#N)C1)C=CC2=CC=C(C=C2)N(C)C)C
Isomeric SMILES:CC1(CC(=CC(=C(C#N)C#N)C1)/C=C/C2=CC=C(C=C2)N(C)C)C

Technology Process of 2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile

There total 6 articles about 2-(3-(4-(Dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-ylidene)malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.5%

: 23051-44-7
3-dicyanomethylidene-1,5,5-trimethylcyclohexene

: 100-10-7
4-dimethylamino-benzaldehyde

: 27334-26-5
2-(3-(2-(4-dimethylaminophenyl)vinyl)-5,5-dimethylcyclohex-2-enylidene)malononitrile

Guidance literature:: With piperidine; In acetonitrile; for 10h; Temperature; Reagent/catalyst; Reflux;

Reference yield: 82.0%

: 23051-44-7
3-dicyanomethylidene-1,5,5-trimethylcyclohexene

: 100-10-7
4-dimethylamino-benzaldehyde

: 27334-26-5
3-(dicyanomethylene)-5,5-dimethyl-1-(4-dimethylamino-styryl) cyclohexene

Guidance literature:: With piperidine; In ethanol; at 85 ℃; for 5h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c01414

Reference yield:

: 78-59-1
3,5,5-Trimethylcyclohex-2-en-1-one

: 27334-26-5
2-(3-(2-(4-dimethylaminophenyl)vinyl)-5,5-dimethylcyclohex-2-enylidene)malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 30 h / Reflux

2: piperidine / ethanol / 20 h / 85 °C

With piperidine; In ethanol;
DOI:10.1002/anie.202103674