(1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

Base Information

Chemical Name:(1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol
CAS No.:1228346-58-4
Molecular Formula:C₂₀H₂₂O₃S
Molecular Weight:342.459
Hs Code.:

Synonyms:(1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

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Chemical Property of (1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

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Technology Process of (1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

There total 2 articles about (1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1228346-59-5
(1R,2S,4S,5S)-4-(benzyloxy)-5-((benzyloxy)methyl)-6-thiabicyclo[3.1.0]hexan-2-yl benzoate

: 1228346-58-4
(1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

Guidance literature:: With ammonia; In methanol; at 40 ℃; for 15h; Sealed tube;
DOI:10.1016/j.tet.2010.02.092

Reference yield: 83.0%

: 1228346-57-3
(1S,2S,4S,5R)-4-((2-methoxyethoxy)methoxy)-2-(benzyloxy)-1-((benzyloxy)methyl)-6-thiabicyclo[3.1.0]hexane

: 1228346-58-4
(1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

Guidance literature:: With toluene-4-sulfonic acid; tert-butyl alcohol; for 8h; Reflux;
DOI:10.1016/j.tet.2010.02.092

Reference yield: 20.0%

: 1228346-58-4
(1R,2S,4S,5S)-4-(benzyloxy)-5-[(benzyloxy)methyl]-6-thiabicyclo[3.1.0]hexan-2-ol

: 65-85-0,8013-63-6
benzoic acid

: 1228346-59-5
(1R,2S,4S,5S)-4-(benzyloxy)-5-((benzyloxy)methyl)-6-thiabicyclo[3.1.0]hexan-2-yl benzoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.092