2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

Base Information

Chemical Name:2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol
CAS No.:503544-29-4
Molecular Formula:C₄₄H₄₀O₁₀Se
Molecular Weight:807.756
Hs Code.:

Synonyms:2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

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Chemical Property of 2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

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Technology Process of 2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

There total 1 articles about 2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 613-90-1
benzoyl cyanide

: 503544-21-6
7,8,9-tri-O-acetyl-2,6-anhydro-4,5-O-carbonylidene-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

: 503544-29-4
2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

: 2,6-anhydro-4,5,7,8,9-penta-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

Guidance literature:: In tetrahydrofuran; triethylamine; at 0 - 5 ℃; for 64h;
DOI:10.1016/S0008-6215(02)00176-3

Reference yield: 99.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 503544-29-4
2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

: 503544-30-7
2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-5-O-trifluoromethanesulfonyl-1-phenylseleno-D-erythro-L-talo-nonitol

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1016/S0008-6215(02)00176-3

Reference yield:

: 503544-29-4
2,6-anhydro-4,7,8,9-tetra-O-benzoyl-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-talo-nonitol

: 2,6-anhydro-5-azido-1,3-dideoxy-2-methyl-1-phenylseleno-D-erythro-L-manno-nonitol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / CH₂Cl₂ / 12 h / 0 - 20 °C

2: 96 percent / tetra-n-butylammonium azide / toluene

3: MeONa / methanol / 12 h / 20 °C

With pyridine; sodium methylate; tetrabutylammoniun azide; In methanol; dichloromethane; toluene;
DOI:10.1016/S0008-6215(02)00176-3