C₂₃H₂₃FN₂O₆S

Base Information

Chemical Name:C₂₃H₂₃FN₂O₆S
CAS No.:1374234-13-5
Molecular Formula:C₂₃H₂₃FN₂O₆S
Molecular Weight:474.51
Hs Code.:

C<sub>23</sub>H<sub>23</sub>FN<sub>2</sub>O<sub>6</sub>S

Synonyms:C₂₃H₂₃FN₂O₆S

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Chemical Property of C₂₃H₂₃FN₂O₆S

Chemical Property:

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Technology Process of C₂₃H₂₃FN₂O₆S

There total 7 articles about C₂₃H₂₃FN₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374234-11-3
C₂₃H₂₄ClFN₂O₆S

: 1374234-13-5
C₂₃H₂₃FN₂O₆S

Guidance literature:: With potassium carbonate; In toluene; at 80 ℃; for 4h;

Reference yield:

: 691857-46-2
ethyl 2-(4-fluorophenyl)-5-hydroxy-6-nitrobenzofuran-3-carboxylate

: 1374234-13-5
C₂₃H₂₃FN₂O₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

2.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

4.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

4.2: 0.5 h / 20 °C

5.1: pyridine / 1 h / 0 - 20 °C

6.1: titanium(IV) isopropylate / tetrahydrofuran / 20 °C / Inert atmosphere

6.2: 2 h / 0 °C

7.1: pyridine / dichloromethane / 2 h / 0 °C

8.1: potassium carbonate / toluene / 4 h / 80 °C

With pyridine; titanium(IV) isopropylate; hydrogenchloride; tin(II) chloride dihdyrate; water; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 691857-07-5
ethyl 2-(4-fluorophenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374234-13-5
C₂₃H₂₃FN₂O₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: boron trichloride / dichloromethane / 1 h / 0 - 20 °C

1.2: Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

3.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

5.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

5.2: 0.5 h / 20 °C

6.1: pyridine / 1 h / 0 - 20 °C

7.1: titanium(IV) isopropylate / tetrahydrofuran / 20 °C / Inert atmosphere

7.2: 2 h / 0 °C

8.1: pyridine / dichloromethane / 2 h / 0 °C

9.1: potassium carbonate / toluene / 4 h / 80 °C

With pyridine; titanium(IV) isopropylate; hydrogenchloride; tin(II) chloride dihdyrate; water; boron trichloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;