1-phenyl-2--3-methylcyclopropene

Base Information

• Chemical Name: 1-phenyl-2--3-methylcyclopropene
• CAS No.: 115757-35-2
• Molecular Formula: C₂₄H₂₂
• Molecular Weight: 310.439

Synonyms:1-phenyl-2--3-methylcyclopropene

Chemical Property of 1-phenyl-2--3-methylcyclopropene

Chemical Property:

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Technology Process of 1-phenyl-2--3-methylcyclopropene

There total 3 articles about 1-phenyl-2--3-methylcyclopropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-Chloro-3-methyl-2-phenyl-cyclopropyl)-2-phenethyl-benzene → 1-phenyl-2--3-methylcyclopropene (115757-35-2)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 0 - 25 ℃; for 13h; Yield given;

DOI:10.1021/jo00253a008

Reference yield:

1--1-propene (115757-33-0,115757-34-1) → 1-phenyl-2--3-methylcyclopropene (115757-35-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 6 h / Heating

2: potassium tert-butoxide / tetrahydrofuran / 13 h / 0 - 25 °C

With potassium tert-butylate; In tetrahydrofuran; benzene;

DOI:10.1021/jo00253a008

Reference yield:

3-chloro-3-phenyl-3H-diazirine (4460-46-2) → 1-phenyl-2--3-methylcyclopropene (115757-35-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 6 h / Heating

2: potassium tert-butoxide / tetrahydrofuran / 13 h / 0 - 25 °C

With potassium tert-butylate; In tetrahydrofuran; benzene;

DOI:10.1021/jo00253a008

upstream raw materials:

1--1-propene

3-chloro-3-phenyl-3H-diazirine

Downstream raw materials:

1-phenyl-2--3,3-dimethylcyclopropene

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