dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester

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Chemical Name:dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester
CAS No.:1057678-18-8
Molecular Formula:C₂₈H₃₀N₆O₂
Molecular Weight:482.585
Hs Code.:

Synonyms:dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester

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Chemical Property of dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester

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Technology Process of dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester

There total 2 articles about dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1057678-14-4
{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}methanol

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1057678-18-8
dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester

Guidance literature:: {6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}methanol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

N,N-Dimethylcarbamoyl chloride; In tetrahydrofuran; at 20 - 60 ℃; for 32h;

With sodium hydride; In tetrahydrofuran;

Reference yield:

: 1057677-65-2
6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]nicotinic acid ethyl ester

: 1057678-18-8
dimethyl-carbamic acid 6-[4-(4-benzyl-phthalazin-1-yl)-piperazin-1-yl]-pyridin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 - 18 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

2.2: 32 h / 20 - 60 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;