N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

Base Information

Chemical Name:N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine
CAS No.:205391-45-3
Molecular Formula:C₂₃H₂₈N₄O₂
Molecular Weight:392.501
Hs Code.:

Synonyms:N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

Chemical Property:

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Technology Process of N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

There total 4 articles about N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.52%

: 4377-33-7
2-chloromethylpyridine

: 158472-17-4
2-{[2-(2-Hydroxy-ethylamino)-ethylamino]-methyl}-phenol

: 205391-45-3
N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

Guidance literature:: With sodium hydroxide; In water;

Reference yield:

: 59488-83-4
N-(salicylideneaminato)-N’-(2-hydroxyethyl)-1,2-ethanediamine

: 205391-45-3
N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 4 h / Cooling with ice

2: sodium hydroxide / 65 °C / pH 10

With sodium tetrahydroborate; sodium hydroxide; In methanol;
DOI:10.1016/j.apcata.2012.12.036

Reference yield:

: 59488-83-4
(E)-2-((2-(2-hydroxyethylamino)ethylimino)methyl)phenol

: 205391-45-3
N-(2-hydroxybenzyl)-N'-(2-hydroxyethyl)-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: 64.52 percent / NaOH / H₂O

With sodium hydroxide; sodium tetrahydroborate; In methanol; water;