C₅₃H₇₀O₉Si

Base Information

Chemical Name:C₅₃H₇₀O₉Si
CAS No.:927662-10-0
Molecular Formula:C₅₃H₇₀O₉Si
Molecular Weight:879.219
Hs Code.:

C<sub>53</sub>H<sub>70</sub>O<sub>9</sub>Si

Synonyms:C₅₃H₇₀O₉Si

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Chemical Property of C₅₃H₇₀O₉Si

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Technology Process of C₅₃H₇₀O₉Si

There total 16 articles about C₅₃H₇₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 927662-09-7
C₅₃H₇₀O₉Si

: 927662-10-0
C₅₃H₇₀O₉Si

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 100 ℃; for 92h;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: C₁₀H₁₆O₅

: 927662-10-0
C₅₃H₇₀O₉Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: NaHMDS / tetrahydrofuran; dimethylformamide / 2 h / 20 °C

1.2: p-TSOH*H₂O / methanol; H₂O; tetrahydrofuran / 0.75 h / 20 °C

1.3: 86 percent / 2,6-lutidine / tetrahydrofuran; dimethylformamide / 0.17 h / 0 °C

2.1: 9-BBN / tetrahydrofuran / 3 h / 20 °C / sonication

2.2: H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 1 h / 20 °C

2.3: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.58 h / 20 °C

3.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

4.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

4.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

5.1: 2-nitrobenzeneselenide; Bu₃P / tetrahydrofuran / 0.42 h / 20 °C

5.2: 77 percent / H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 3.5 h / 45 °C

6.1: 89 percent / DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

7.1: 76 percent / MeLi / tetrahydrofuran / 1 h / -78 - 20 °C

8.1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

9.1: 67 percent / ruthenium ethylidene complex / toluene / 100 °C

10.1: 73 percent / H₂ / PtO₂ / ethyl acetate / 3 h / 20 °C

11.1: 84 percent / DBU / toluene / 92 h / 100 °C

With 9-borabicyclo[3.3.1]nonane dimer; tributylphosphine; methyllithium; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; scandium tris(trifluoromethanesulfonate); platinum(IV) oxide; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: 927661-98-1
C₃₁H₄₅NO₄Si

: 927662-10-0
C₅₃H₇₀O₉Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: DIBAL-H / CH₂Cl₂ / -78 °C

1.2: NaBH₄ / ethanol / 1.5 h / 20 °C

1.3: 78 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

2.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

3.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

3.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

4.1: 2-nitrobenzeneselenide; Bu₃P / tetrahydrofuran / 0.42 h / 20 °C

4.2: 77 percent / H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 3.5 h / 45 °C

5.1: 89 percent / DIBAL-H / CH₂Cl₂ / 0.5 h / -78 °C

6.1: 76 percent / MeLi / tetrahydrofuran / 1 h / -78 - 20 °C

7.1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 20 °C

8.1: 67 percent / ruthenium ethylidene complex / toluene / 100 °C

9.1: 73 percent / H₂ / PtO₂ / ethyl acetate / 3 h / 20 °C

10.1: 84 percent / DBU / toluene / 92 h / 100 °C

With tributylphosphine; methyllithium; hydrogen; diisobutylaluminium hydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; scandium tris(trifluoromethanesulfonate); platinum(IV) oxide; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; benzene;
DOI:10.3987/COM-06-S(O)23