C₅₆H₈₀O₉Si₂

Base Information

Chemical Name:C₅₆H₈₀O₉Si₂
CAS No.:1391927-64-2
Molecular Formula:C₅₆H₈₀O₉Si₂
Molecular Weight:953.417
Hs Code.:

C<sub>56</sub>H<sub>80</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₅₆H₈₀O₉Si₂

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Chemical Property of C₅₆H₈₀O₉Si₂

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Technology Process of C₅₆H₈₀O₉Si₂

There total 15 articles about C₅₆H₈₀O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391927-59-5
C₅₄H₇₆O₈Si₂

: 107-30-2
chloromethyl methyl ether

: 1391927-64-2
C₅₆H₈₀O₉Si₂

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 35 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ol301795a

Reference yield:

: (2S)-4-benzyloxy-2-(4-methoxybenzyloxy)-butyraldehyde

: 1391927-64-2
C₅₆H₈₀O₉Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium bromide diethyl etherate / dichloromethane / -78 - 0 °C / Inert atmosphere

2: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 35 °C / Inert atmosphere

With magnesium bromide diethyl etherate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol301795a

Reference yield:

: 92512-41-9
C₂₁H₂₈O₃Si

: 1391927-64-2
C₅₆H₈₀O₉Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 - -55 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: 0.33 h / -78 °C / Inert atmosphere

3.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 5 h / 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / methanol / 22 h / 40 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

6.1: tetrahydrofuran / -78 °C / Inert atmosphere

6.2: 1 h / 20 °C / Molecular sieve; Inert atmosphere

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C

8.1: 1H-imidazole; dmap / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

9.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.67 h / -78 °C / Inert atmosphere

9.2: 0.83 h / -78 °C / Inert atmosphere

10.1: magnesium bromide diethyl etherate / dichloromethane / -78 - 0 °C / Inert atmosphere

11.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 35 °C / Inert atmosphere

With 1H-imidazole; dmap; n-butyllithium; tetrapropylammonium perruthennate; magnesium bromide diethyl etherate; water; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium hexamethylsilazane; sodium hydride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene;
DOI:10.1021/ol301795a