[13C^α]GlyNHBn

Base Information

• Chemical Name: [13C^α]GlyNHBn
• CAS No.: 905992-12-3
• Molecular Formula: C₉H₁₂N₂O
• Molecular Weight: 165.196
• Mol file: 905992-12-3.mol

Synonyms:[13C^α]GlyNHBn

Chemical Property of [13C^α]GlyNHBn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [13C^α]GlyNHBn

There total 2 articles about [13C^α]GlyNHBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

[2-13C]-2-azido-N-benzyl-acetamide → [13Cα]GlyNHBn (905992-12-3)

Guidance literature:

With ethyl-diphenyl-phosphane; In tetrahydrofuran; for 8h;

DOI:10.1021/ja060484k

Reference yield:

[2-13C]-2-azido-N-benzyl-acetamide + acetylamino-thioacetic acid S-(2-diphenylphosphanyl-phenyl) ester (289038-93-3) → [13Cα]GlyNHBn (905992-12-3) + AcGly[13Cα]GlyNHBn

Guidance literature:

In water-d2; N,N-dimethyl-formamide; Kinetics;

DOI:10.1021/ja060484k

Reference yield: 81.0%

[13Cα]GlyNHBn (905992-12-3) + Diphenylphosphinic chloride (1499-21-4) → Ph2P(O)[13Cα]GlyNHBn

Guidance literature:

With dmap; In tetrahydrofuran; for 8h;

DOI:10.1021/ja060484k

upstream raw materials:

acetylamino-thioacetic acid S-(2-diphenylphosphanyl-phenyl) ester