3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

Base Information

Chemical Name:3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate
CAS No.:1541178-86-2
Molecular Formula:C₃₂H₃₂F₃NO₈
Molecular Weight:615.603
Hs Code.:

Synonyms:3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

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Chemical Property of 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

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Technology Process of 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

There total 2 articles about 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,6-di-O-acetyl-2,4-di-O-benzyl-D-glucopyranose

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1541178-86-2
3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

: 1541178-87-3
O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Guidance literature:: With potassium carbonate; In acetone; Overall yield = 86 %; Overall yield = 121 mg;
DOI:10.1016/j.carres.2013.11.016

Reference yield:

: 1541178-84-0
3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranose

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1541178-86-2
3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

: 1541178-87-3
O-(3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Guidance literature:: With potassium carbonate; In acetone; for 3h; Overall yield = 95 percent; Overall yield = 626 mg; Inert atmosphere;
DOI:10.1039/d0ob01776k

Reference yield:

: 1541178-94-2
C₃₄H₃₄O₈

: 1541178-86-2
3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl N-phenyl-2,2,2-trifluoroacetimidate

: 1541179-36-5
p-methoxyphenyl 3,6-di-O-acetyl-2,4-di-O-benzyl-α-D-glucopyranosyl-(1→6)-3-O-benzoyl-2,4-di-O-benzyl-β-D-glucopyranoside

: 1541179-38-7
p-methoxyphenyl 3,6-di-O-acetyl-2,4-di-O-benzyl-β-D-glucopyranosyl-(1→6)-3-O-benzoyl-2,4-di-O-benzyl-β-D-glucopyranoside

Guidance literature:: With methyl trifluoromethanesulfonate; In dichloromethane; at -35 - -15 ℃; for 0.583333h; Overall yield = 93 %; Molecular sieve;
DOI:10.1016/j.carres.2013.11.016