N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

Base Information

Chemical Name:N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide
CAS No.:882408-53-9
Molecular Formula:C₂₀H₃₃N₃O₃Si₂
Molecular Weight:419.671
Hs Code.:

Synonyms:N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

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Technology Process of N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

There total 1 articles about N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 882408-58-4
(bis-trimethylsilanyl-methyl)-phenethyl-amine

: 57072-87-4
chlorocarbonyl-diazo-acetic acid ethyl ester

: 882408-53-9
N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2005.12.020

Reference yield: 92.0%

: 882408-53-9
N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

: 1-bis(trimethylsilyl)methyl-3-ethoxycarbonyl-4-phenyl-2-pyrrolidinone

Guidance literature:: With dirhodium(II) tetrakis; In dichloromethane; at 45 ℃;
DOI:10.1016/j.tetasy.2005.12.020

Reference yield:

: 882408-53-9
N-bis(trimethylsilyl)methyl-N-phenethyl-α-carboethoxy-α-diazoacetamide

: 1-bis(trimethylsilyl)methyl-3-ethoxycarbonyl-4-phenyl-2-pyrrolidinone

: 2-benzyl-1-(bis-trimethylsilanyl-methyl)-4-oxo-azetidine-3-carboxylic acid ethyl ester

Guidance literature:: With dirhodium(II) tetrakis[(S)-N-phthaloyl-tert-leucinate]; In dichloromethane; at 45 ℃; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2005.12.020