Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt

Base Information

Chemical Name:Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt
CAS No.:1374460-69-1
Molecular Formula:C₂₆H₃₄N₂P₂Zn
Molecular Weight:501.907
Hs Code.:

Synonyms:Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt

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Chemical Property of Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt

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Technology Process of Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt

There total 4 articles about Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1100362-71-7
(diphenylphosphanyl)(phenyl(isopropylamino)phosphanyl)(isopropyl)amine

: 557-20-0
diethylzinc

: 1374460-69-1
Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt

Guidance literature:: In diethyl ether; toluene; at 20 ℃; for 12h;

Reference yield: 65.0%

: 1100362-71-7
(diphenylphosphanyl)(phenyl(isopropylamino)phosphanyl)(isopropyl)amine

: 557-20-0
diethylzinc

: 1374460-69-1
[((C₆H₅)2PN(CH(CH₃)2)P(C₆H₅)NCH(CH₃)2)Zn(C₂H₅)]

Guidance literature:: In diethyl ether; toluene; byproducts: C2H6; (Ar); std. Schlenk technique; soln. of Zn compd. in toluene was added tosoln. of ligand in Et2O at room temp.; stirred for 12 h; concd.; cooled to -30°C; elem. anal.;
DOI:10.1021/om300186a

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 1374460-69-1
Ph₂PN(i-Pr)P(Ph)N(i-Pr)ZnEt

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 72.5 h / 0 °C

2: triethylamine / tetrahydrofuran / 24 h / -40 - 20 °C

3: diethyl ether; toluene / 12 h / 20 °C

With triethylamine; In tetrahydrofuran; diethyl ether; toluene;