Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Base Information

Chemical Name:Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester
CAS No.:193952-84-0
Molecular Formula:C₄₂H₄₂O₁₂
Molecular Weight:738.788
Hs Code.:

Synonyms:Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

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Chemical Property of Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

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Technology Process of Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

There total 1 articles about Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4422-95-1
1,3,5-benzene tris(carbonyl chloride)

: 88280-53-9
(R)-3-hydroxybutanoic benzyl ester

: 193952-84-0
Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Guidance literature:: With pyridine; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1002/hlca.19970800402

Reference yield: 97.0%

: 193952-84-0
Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

: 183058-30-2
Benzene-1,3,5-tricarboxylic acid tris-((R)-2-carboxy-1-methyl-ethyl) ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1002/hlca.19970800402

Reference yield:

: 193952-84-0
Benzene-1,3,5-tricarboxylic acid tris-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

: Benzene-1,3,5-tricarboxylic acid tris-((R)-2-chlorocarbonyl-1-methyl-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / H₂ / 10 percent Pd/C / methanol; various solvent(s)

2: oxalyl chloride / CH₂Cl₂; ethyl acetate / Ambient temperature

With oxalyl dichloride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19970800402