N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

Base Information

Chemical Name:N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide
CAS No.:1616475-43-4
Molecular Formula:C₂₄H₂₄N₄O₂
Molecular Weight:400.48
Hs Code.:

Synonyms:N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

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Chemical Property of N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

Chemical Property:

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Technology Process of N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

There total 5 articles about N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₆N₄O₂S

: 1616475-43-4
N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

Guidance literature:: With potassium carbonate; diisopropyl-carbodiimide; In acetonitrile; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.05.009

Reference yield:

: 1616475-37-6
4-(2-(dimethylamino)ethoxy)-2-nitro-N-phenylaniline

: 1616475-43-4
N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 1.5 h / 20 °C / 760.05 Torr / Inert atmosphere

2: acetonitrile / 2 h / 20 °C / Inert atmosphere

3: potassium carbonate; diisopropyl-carbodiimide / acetonitrile / 20 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; potassium carbonate; diisopropyl-carbodiimide; In methanol; acetonitrile;
DOI:10.1016/j.bmcl.2014.05.009

Reference yield:

: 1616475-30-9
2-(4-chloro-3-nitrophenoxy)-N,N-dimethylethanamine

: 1616475-43-4
N-(5-(2-(dimethylamino)ethoxy)-1-phenyl-1H-benzo[d]imidazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 28 h / Inert atmosphere; Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 1.5 h / 20 °C / 760.05 Torr / Inert atmosphere

3: acetonitrile / 2 h / 20 °C / Inert atmosphere

4: potassium carbonate; diisopropyl-carbodiimide / acetonitrile / 20 h / 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; diisopropyl-carbodiimide; In methanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2014.05.009