Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

Base Information

Chemical Name:Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate
CAS No.:111923-96-7
Molecular Formula:C₃₄H₃₈N₂O₇S
Molecular Weight:618.751
Hs Code.:

Synonyms:Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

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Technology Process of Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

There total 3 articles about Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 111923-96-7
Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

Guidance literature:

Reference yield:

: 34097-60-4
methyl benzenesulfonylacetate

: 104448-45-5
4-<<6-(2-ethylhexanamido)indol-1-yl>methyl>-3-methoxybenzoic N,N-diphenylcarbamic anhydride

: 111923-96-7
Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 2.) from -78 deg C to RT, overnight;
DOI:10.1021/jm00171a018

Reference yield:

: 104436-22-8
4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoic acid

: 111923-96-7
Methyl 2-[4-[6-(2-ethylhexanamido)indol-1-ylmethyl]-3-methoxybenzoyl]-2-phenylsulphonylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Et₃N / methanol

2: 1.) LDA / 1.) THF, -78 deg C, 2.) from -78 deg C to RT, overnight

With triethylamine; lithium diisopropyl amide; In methanol;
DOI:10.1021/jm00171a018