Technology Process of C38H50O4Si2
There total 9 articles about C38H50O4Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide;
In
acetonitrile;
at 0 ℃;
for 1h;
Molecular sieve;
Inert atmosphere;
DOI:10.1021/ja411270d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / chloroform / 20 °C / Inert atmosphere
2: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / acetonitrile / 1 h / 0 °C / Molecular sieve; Inert atmosphere
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; trifluoroacetic acid;
In
chloroform; acetonitrile;
DOI:10.1021/ja411270d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: isopropyl alcohol; diethylzinc; ((2S,2'S)-((2-hydroxy-5-methyl-1,3-phenylene)bis(methylene))bis(pyrrolidine-1,2-diyl))bis(diphenylmethanol) / tetrahydrofuran / 72 h / -20 °C / Inert atmosphere; Molecular sieve
2: diethyl methoxy borane; sodium tetrahydroborate / Inert atmosphere
3: pyridine / Inert atmosphere
4: trifluoroacetic acid / chloroform / 20 °C / Inert atmosphere
5: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / Inert atmosphere
With
pyridine; sodium tetrahydroborate; tetrapropylammonium perruthennate; diethyl methoxy borane; diethylzinc; 4-methylmorpholine N-oxide; isopropyl alcohol; trifluoroacetic acid; ((2S,2'S)-((2-hydroxy-5-methyl-1,3-phenylene)bis(methylene))bis(pyrrolidine-1,2-diyl))bis(diphenylmethanol);
In
tetrahydrofuran; chloroform;
5: |Ley Oxidation;
DOI:10.1021/jacs.6b05127
