2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

Base Information

Chemical Name:2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester
CAS No.:1432752-40-3
Molecular Formula:C₁₅H₁₉NO₅
Molecular Weight:293.32
Hs Code.:

Synonyms:2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

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Chemical Property of 2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

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Technology Process of 2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

There total 5 articles about 2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

: 255376-41-1
5-methoxy-2-methoxycarbonylmethyl-benzoic acid methyl ester

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 1432752-40-3
2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

Guidance literature:: With acetic acid; at 90 ℃; for 12h;

Reference yield:

: 1370606-52-2
2-(2-carboxy-4-methoxy-phenyl)-malonic acid dimethyl ester

: 1432752-40-3
2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: water; lithium hydroxide / methanol / 12 h / 40 °C

2: toluene / 12 h / 105 °C

3: thionyl chloride / methanol / 12 h / 65 °C

4: acetic acid / 12 h / 90 °C

With thionyl chloride; water; acetic acid; lithium hydroxide; In methanol; toluene;

Reference yield:

: 1432752-19-6
2-(2-carboxy-4-methoxy-phenyl)-malonic acid

: 1432752-40-3
2-(2-dimethylamino-1-methoxycarbonyl-vinyl)-5-methoxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 12 h / 105 °C

2: thionyl chloride / methanol / 12 h / 65 °C

3: acetic acid / 12 h / 90 °C

With thionyl chloride; acetic acid; In methanol; toluene;