[5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

Base Information

Chemical Name:[5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane
CAS No.:206255-19-8
Molecular Formula:C₃₉H₄₃OPSi
Molecular Weight:586.829
Hs Code.:

[5-(<i>tert</i>-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ<sup>5</sup>-phosphane

Synonyms:[5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

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Chemical Property of [5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

Chemical Property:

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Technology Process of [5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

There total 6 articles about [5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [5-(tert-butyldiphenylsilyloxy)pentyl]triphenylphosphonium iodide

: 206255-19-8
[5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

Guidance literature:: In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;
DOI:10.1021/jo048681u

Reference yield:

: 111-29-5
1 ,5-pentanediol

: 206255-19-8
[5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / dimethylformamide

2: Et₃N / CH₂Cl₂

3: NaI / acetone

4: 2.) KN(TMS)2 / 1.) PhH; 2.) THF, -78 deg C

With 1H-imidazole; potassium hexamethylsilazane; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(98)00279-2

Reference yield:

: 121671-76-9
5-(tert-butyldiphenylsilyloxy)pentan-1-ol

: 206255-19-8
[5-(tert-butyl-diphenyl-silanyloxy)-pentylidene]-triphenyl-λ⁵-phosphane

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂

2: NaI / acetone

3: 2.) KN(TMS)2 / 1.) PhH; 2.) THF, -78 deg C

With potassium hexamethylsilazane; triethylamine; sodium iodide; In dichloromethane; acetone;
DOI:10.1016/S0040-4039(98)00279-2