phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside
CAS No.:362614-09-3
Molecular Formula:C₃₂H₃₁NO₉S
Molecular Weight:605.665
Hs Code.:

Synonyms:phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

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Chemical Property of phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

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Technology Process of phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

There total 5 articles about phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-24-7
acetic anhydride

: 362614-08-2
phenyl 2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

: 362614-09-3
phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 8h;
DOI:10.1081/CAR-100103959

Reference yield:

: 81704-02-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-galactopyranoside

: 362614-09-3
phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 97 percent / BF₃*OEt₂ / CH₂Cl₂ / 24 h / 20 °C

2.1: 98 percent / MeONa / methanol / 5 h / 20 °C

3.1: dibutyltin oxide / methanol / 5 h / Heating

3.2: 58 percent / Bu₄NBr / benzene / 1 h / Heating

4.1: 99 percent / pyridine / 8 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; sodium methylate; di(n-butyl)tin oxide; In methanol; dichloromethane;
DOI:10.1081/CAR-100103959

Reference yield:

: 108-98-5
thiophenol

: 362614-09-3
phenyl 4,6-di-O-acetyl-2-deoxy-3-O-p-methoxybenzyl-2-phthalimido-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 97 percent / BF₃*OEt₂ / CH₂Cl₂ / 24 h / 20 °C

2.1: 98 percent / MeONa / methanol / 5 h / 20 °C

3.1: dibutyltin oxide / methanol / 5 h / Heating

3.2: 58 percent / Bu₄NBr / benzene / 1 h / Heating

4.1: 99 percent / pyridine / 8 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; sodium methylate; di(n-butyl)tin oxide; In methanol; dichloromethane;
DOI:10.1081/CAR-100103959