(2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

Base Information

Chemical Name:(2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol
CAS No.:100569-41-3
Molecular Formula:C₁₆H₂₆O₇
Molecular Weight:330.378
Hs Code.:

Synonyms:(2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

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Technology Process of (2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

There total 4 articles about (2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100569-42-4
(2S,3S,4S)-5-(benzyloxy)-3,4-bis<(methoxymethyl)oxy>-1-(4-methoxyphenyl)-2-propanol

: 100569-41-3
(2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 1h; under 760 Torr;
DOI:10.1021/jo00357a023

Reference yield: 81.0%

: (3R,4S,5S)-5-(4-Methoxy-benzyl)-3,4-bis-methoxymethoxy-dihydro-furan-2-one

: 100569-41-3
(2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

Guidance literature:: With diisobutylaluminium hydride; In toluene; benzene; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2004.09.012

Reference yield:

: 252911-88-9
(3R,4R,5S)-3,4-Dihydroxy-5-(4-methoxy-benzyl)-dihydro-furan-2-one

: 100569-41-3
(2S,3S,4S)-2,3-bis<(methoxymethyl)oxy>-5-(4-methoxyphenyl)-1,4-pentanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / i-Pr₂NEt / acetonitrile / 24 h / 20 °C

2: 81 percent / Dibal-H / benzene; toluene / 1 h / 0 °C

With diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; In toluene; acetonitrile; benzene;
DOI:10.1016/j.tet.2004.09.012