2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

Base Information

Chemical Name:2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester
CAS No.:1609182-79-7
Molecular Formula:C₁₃H₁₃NO₂S₂
Molecular Weight:279.384
Hs Code.:

Synonyms:2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

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Chemical Property of 2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

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Technology Process of 2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

There total 3 articles about 2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: C₁₃H₁₄OS₂

: 1609182-79-7
2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

Guidance literature:: With hydrogenchloride; sodium nitrite; In methanol; at 0 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/acs.joc.7b01601

Reference yield: 79.0%

: 1599485-52-5
C₁₃H₁₄OS₂

: 1609182-79-7
2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

Guidance literature:: With hydrogenchloride; sodium nitrite; In methanol; for 0.166667h; Cooling with ice;
DOI:10.1016/j.tet.2014.03.097

Reference yield:

: 63297-99-4
trithiocarbonic acid bis-(2-methyl-allyl) ester

: 1609182-79-7
2-hydroxyimino-3-oxo-3-phenyl-dithiopropionic acid 2-methyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 °C / Inert atmosphere

2.1: hydrogenchloride; sodium nitrite / methanol / 0.08 h / 0 °C / Inert atmosphere

With hydrogenchloride; sodium hydride; sodium nitrite; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/acs.joc.7b01601