Technology Process of 1,2-dicyano-4,5-diheptylbenzene
There total 5 articles about 1,2-dicyano-4,5-diheptylbenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0);
In
N,N-dimethyl-formamide;
at 20 - 63 ℃;
for 6h;
Inert atmosphere;
DOI:10.1142/S108842461350020X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / diethyl ether / 0.5 h / 20 °C / Inert atmosphere
2: acetic acid; hydrogen bromide / 18 h / Reflux
3: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere
4: bis(dibenzylideneacetone)-palladium(0); 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 6 h / 20 - 63 °C / Inert atmosphere
With
2,6-dimethylpyridine; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; hydrogen bromide; acetic acid; bis(dibenzylideneacetone)-palladium(0);
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1142/S108842461350020X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / diethyl ether / 0.5 h / 20 °C / Inert atmosphere
2: acetic acid; hydrogen bromide / 18 h / Reflux
3: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere
4: bis(dibenzylideneacetone)-palladium(0); 1,1'-bis-(diphenylphosphino)ferrocene / N,N-dimethyl-formamide / 6 h / 20 - 63 °C / Inert atmosphere
With
2,6-dimethylpyridine; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; hydrogen bromide; acetic acid; bis(dibenzylideneacetone)-palladium(0);
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1142/S108842461350020X
