phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

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Chemical Name:phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside
CAS No.:1133292-35-9
Molecular Formula:C₅₀H₅₁FO₇SSi
Molecular Weight:843.101
Hs Code.:

Synonyms:phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1133292-22-4
4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl bromide

: 808762-00-7
phenyl 4,6-O-benzylidene-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

: 1133292-35-9
phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

Guidance literature:: phenyl 4,6-O-benzylidene-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; Inert atmosphere;

4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jo900026e

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1133292-35-9
phenyl 4,6-O-benzylidene-3-O-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl]-2-O-(4-methoxybenzyl)-1-thio-α-D-mannopyranoside

: C₄₅H₄₆F₄O₁₀SSi

Guidance literature:: With 1-benzenesulfinyl piperidine; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.5h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo900026e