C₃₃H₅₂O₇

Base Information

Chemical Name:C₃₃H₅₂O₇
CAS No.:1610421-87-8
Molecular Formula:C₃₃H₅₂O₇
Molecular Weight:560.772
Hs Code.:

C<sub>33</sub>H<sub>52</sub>O<sub>7</sub>

Synonyms:C₃₃H₅₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₅₂O₇

Chemical Property:

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Technology Process of C₃₃H₅₂O₇

There total 12 articles about C₃₃H₅₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610421-86-7
C₃₉H₆₆O₇Si

: 1610421-87-8
C₃₃H₅₂O₇

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2014.04.040

Reference yield:

: 1072455-36-7
methyl (5Z,8R)-8,9-dihydroxynon-5-enoate

: 1610421-87-8
C₃₃H₅₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 0 °C

2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 24 h / -10 °C

3.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C

3.2: -30 °C

4.1: triethylamine; lithium bromide / tetrahydrofuran / 1.5 h / 20 °C

4.2: 20 °C

5.1: cerium(III) chloride heptahydrate / methanol / 0.08 h / 20 °C

5.2: 1 h / -78 °C

6.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C

With 1H-imidazole; oxalyl dichloride; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; pyridine hydrogenfluoride; dimethyl sulfoxide; triethylamine; lithium bromide; In tetrahydrofuran; pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.04.040

Reference yield:

: 98314-97-7
(Z)-2-octenyl iodide

: 1610421-87-8
C₃₃H₅₂O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

1.2: -78 - -40 °C

2.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 3 h / 0 °C

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

4.2: 6 h / -78 °C

5.1: triethylamine; lithium bromide / tetrahydrofuran / 1.5 h / 20 °C

5.2: 20 °C

6.1: cerium(III) chloride heptahydrate / methanol / 0.08 h / 20 °C

6.2: 1 h / -78 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C

With dmap; n-butyllithium; lithium hydroxide monohydrate; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; triethylamine; dicyclohexyl-carbodiimide; lithium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1016/j.tet.2014.04.040