(2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

Base Information

Chemical Name:(2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one
CAS No.:781647-75-4
Molecular Formula:C₂₄H₂₉NO₈
Molecular Weight:459.496
Hs Code.:

Synonyms:(2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

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Chemical Property of (2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

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Technology Process of (2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

There total 1 articles about (2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 81036-97-7
(2S,5S)-2-tert-butyl-5-phenyl-1,3-dioxolan-4-one

: 1-fluoro-2-(2-methoxy-ethoxymethoxymethyl)-4-nitro-benzene

: 781647-75-4
(2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

Guidance literature:: (2S,5S)-2-tert-butyl-5-phenyl-1,3-dioxolan-4-one; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃;

1-fluoro-2-(2-methoxy-ethoxymethoxymethyl)-4-nitro-benzene; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃;
DOI:10.1055/s-2003-42123

Reference yield: 80.0%

: 781647-75-4
(2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

: 781647-89-0
(R)-2-methoxyethoxymethoxymethyl-4-nitrobenzilic acid

Guidance literature:: With potassium hydroxide; In ethanol; at 20 ℃;
DOI:10.1055/s-2003-42123 DOI:10.1021/jo0402069

Reference yield:

: 781647-75-4
(2S,5R)-2-tert-butyl-5-(2-methoxyethoxymethoxymethyl-4-nitrophenyl)-5-phenyl-1,3-dioxolan-4-one

: 2-methoxyethoxymethoxymethyl-4-nitrobenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / KOH / ethanol / 20 °C

2: 65 percent / O₂; pivalaldehyde; substituted o-phenylenediamine Co(III) complex / acetonitrile

With potassium hydroxide; substituted o-phenylenediamine Co(III); oxygen; pivalaldehyde; In ethanol; acetonitrile;
DOI:10.1021/jo0402069