1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

Base Information

Chemical Name:1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran
CAS No.:86146-30-7
Molecular Formula:C₂₉H₃₆O₅
Molecular Weight:464.602
Hs Code.:

1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzo<b,d>pyran

Synonyms:1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

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Chemical Property of 1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

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Technology Process of 1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

There total 4 articles about 1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 86146-28-3
1-Methoxy-3,6,6,9-tetramethyl-7,8,9,10-tetrahydro-(6H)-dibenzo-2-pyranyl-methanphosphonsaeurediethylester

: 86146-30-7
1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

Guidance literature:: With potassium tert-butylate; In benzene;
DOI:10.1002/ardp.19833160408

Reference yield:

: 86146-25-0
1-Hydroxy-2-hydroxymethyl-3,6,6,9-tetramethyl-7,8,9,10-tetrahydro-(6H)-dibenzopyran

: 86146-30-7
1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / cyclohexane / 20 h / 40 °C

2: 85 percent / diethyl ether

3: 73 percent / t-BuOK / benzene

With potassium tert-butylate; In diethyl ether; cyclohexane; benzene;
DOI:10.1002/ardp.19833160408

Reference yield:

: 86146-26-1
1-Hydroxy-3,6,6,9-tetramethyl-7,8,9,10-tetrahydro-(6H)-dibenzopyran-2-yl-methanphosphonsaeurediethylester

: 86146-30-7
1-Methoxy-3,6,6,9-tetramethyl-2-(3,4,5-trimethoxystyryl)-7,8,9,10-tetrahydro-(6H)-dibenzopyran

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / diethyl ether

2: 73 percent / t-BuOK / benzene

With potassium tert-butylate; In diethyl ether; benzene;
DOI:10.1002/ardp.19833160408