diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

Base Information

Chemical Name:diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate
CAS No.:939387-58-3
Molecular Formula:C₂₃H₂₇F₃NO₅P
Molecular Weight:485.44
Hs Code.:

Synonyms:diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

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Chemical Property of diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

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Technology Process of diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

There total 1 articles about diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 939387-57-2
diethyl (E)-3-[N-acetyl-N-(benzyloxy)amino]-1-(tributylstannyl)prop-1-enylphosphonate

: 455-13-0
4-Iodobenzotrifluoride

: 939387-58-3
diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

Guidance literature:: With copper(l) iodide; trifuran-2-yl-phosphane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In 1-methyl-pyrrolidin-2-one; at 20 ℃;
DOI:10.1021/jo0700981

Reference yield: 85.0%

: 939387-58-3
diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

: 939387-59-4
diethyl 3-[N-acetyl-N-(hydroxy)amino]-1-(4-trifluoromethylphenyl)propylphosphonate

Guidance literature:: With hydrogen; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 4h; atmospheric pressure;
DOI:10.1021/jo0700981

Reference yield:

: 939387-58-3
diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(4-trifluoromethylphenyl)propenylphosphonate

: 3-[N-acetyl-N-(hydroxy)amino]-1-(4-trifluoromethylphenyl)propylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / H₂; Na₂CO₃ / Pd/C / tetrahydrofuran / 4 h / 20 °C / atmospheric pressure

2: 23 percent / TMSBr / acetonitrile / 48 h / 20 °C

With trimethylsilyl bromide; hydrogen; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo0700981