(E)-O-cinnamyl benzylcarbamothioate

Base Information

Chemical Name:(E)-O-cinnamyl benzylcarbamothioate
CAS No.:1228453-84-6
Molecular Formula:C₁₇H₁₇NOS
Molecular Weight:283.394
Hs Code.:

Synonyms:(E)-O-cinnamyl benzylcarbamothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-O-cinnamyl benzylcarbamothioate

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Technology Process of (E)-O-cinnamyl benzylcarbamothioate

There total 2 articles about (E)-O-cinnamyl benzylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 622-78-6
Benzyl isothiocyanate

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 1228453-84-6
(E)-O-cinnamyl benzylcarbamothioate

Guidance literature:: (2E)-3-phenyl-2-propen-1-ol; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Benzyl isothiocyanate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo1006152

Reference yield: 38.0%

: C₁₇H₁₅NOS

: 1228453-84-6
(E)-O-cinnamyl benzylcarbamothioate

Guidance literature:: With formaldehyd; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; water; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 80 ℃; stereoselective reaction;
DOI:10.1002/cctc.202001411

Reference yield: 14.0%

: 1228453-84-6
(E)-O-cinnamyl benzylcarbamothioate

: C₁₇H₁₇NOS

: 1228453-96-0
C₁₇H₁₇NOS

: C₁₇H₁₇NOS

Guidance literature:: With propylamine; O,O'-(S)-(1,1'-dinaphthyl-2,2'-diyl)-N,N-di-(S,S)-[2-phenylethylphosphoramidite]; bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium acetate; In 1,4-dioxane; at 50 ℃; optical yield given as %ee; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo1006152